2,3-Dichlorobenzoic acid → HCID 73673187, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,3-dichlorobenzoic acid and 3-cyclopropyl-2-(2-methylpyrimidin-5-yl)propan-1-amine was separated into the two enantiomers by preparative SFC to yield the title compound LCMS (MH+): m/z=364.1, tR (minutes, Method F)=2.64. [α]D20=+41.3 (c=1.5 mg/mL,CHCl3)

Provenance & Evidence