2,6-Dichlorobenzoic acid → HCID 73673190, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,6-dichlorobenzoic acid and 3-cyclopropyl-2-(2-methylpyrimidin-5-yl)propan-1-amine was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=364.1, tR (minutes, Method F)=2.43. [α]D20=+15.42 (c=2.4 mg/mL,CHCl3)

Provenance & Evidence