2,3-Dichlorobenzoic acid → HCID 73673306, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,3-dichlorobenzoic acid and 3-(1-(trifluoromethyl)cyclopropyl)-2-(2-(trifluoromethyl)pyrimidin-5-yl)propan-1-amine was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=486.1, tR (minutes, Method F)=2.77. [α]D20==+31.03 (c=5.80 mg/mL,CHCl3)

Provenance & Evidence