2,3-Dichlorobenzoic acid → HCID 73673307, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,3-dichlorobenzoic acid and 3-(1-(trifluoromethyl)cyclopropyl)-2-(2-(trifluoromethyl)pyridin-5-yl)propan-1-amine was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=485.1, tR (minutes, Method G)=2.63. [α]D20=+27.63 (c=1.52 mg/mL,CHCl3)

Provenance & Evidence