2,6-Dichlorobenzoic acid → HCID 86716424, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,6-dichlorobenzoic acid and 2-phenyl-2-(6-(trifluoromethyl)pyridin-3-yl)ethanamine was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=439.1, tR (minutes, Method G)=2.76. [α]D20=+3.18 (c=6.38 mg/mL,CHCl3)

Provenance & Evidence