2,3-Dichlorobenzoic acid → HCID 86716375, compound

Participants

Reaction Steps

The racemic mixture which was prepared in a similar manner to example 3a from 2,3-dichlorobenzoic acid and 2-(4-fluorophenyl)-2-(6-(trifluoromethyl)pyridin-3-yl)ethanamine was separated into the two enantiomers by preparative SFC to yield the title compound. LCMS (MH+): m/z=457.0, tR (minutes, Method G)=3.02. [α]D20=+4.17 (c=3.04 mg/mL,CHCl3) And the corresponding enantiomer

Provenance & Evidence