HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Bromo-3,5-dimethoxyphenyl)furan → HCID 58432156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Bromo-3,5-dimethoxyphenyl)furan | HCID 58431988 | — |
| Reactant | 2-(cyclopropylmethoxy)-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide | HCID 58431995 | — |
| Product | HCID 58432156 | HCID 58432156 | — |
Reaction Steps
1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(cyclopropylmethoxy)-2-(4-morpholinophenyl)ethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-(cyclopropylmethoxy)-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (40% EtOAc/hexanes) gave the product as a pale yellow solid (0.092 g, 23% yield). MS: m/z 556.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102643B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-3e7aecefc6394930bef55c9bd755478b |
| Source note | uspto-grants-2015_08 |