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HRID512698

反应详情

EQUATION

反应方程式

HRID 512698 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(-c2ccco2)cc(OC)c1Cl
HCID58432088

未命名化合物

结构：CCOC(C(=O)N(C)OC)c1ccc(N2CCOCC2)cc1
HCID58432131

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(C(=O)c1ccc(-c2cc(OC)c(Cl)c(OC)c2)o1)c1ccc(N2CCOCC2)cc1
HCID58432137

未命名化合物

PROCEDURE

实验过程

1-(5-(4-Chloro-3,5-dimethoxyphenyl)furan-2-yl)-2-ethoxy-2-(4-morpholinophenyl)ethanone was prepared from 2-(4-chloro-3,5-dimethoxyphenyl)furan and 2-ethoxy-N-methoxy-N-methyl-2-(4-morpholinophenyl)acetamide according to the procedure used in Example 30. Purification by chromatography (60% EtOAc-hexanes) gave the product as a pale yellow solid (0.127 g, 26% yield). MS: m/z 486.5 [M+H]+.

WORKUP

后处理

  1. customPurification by chromatography (60% EtOAc-hexanes)