Aniline → HCID 57023940, compound

HRID 5132Notes

Reaction equation

HRID 5132 reaction equation
[CH2:1]1[C:13]2[C:12]3[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=3[N:6]=[CH:5][C:4]=2[C:3](=[O:14])O1.[NH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>CCCCCC>[C:16]1([N:15]2[CH2:1][C:13]3[C:12]4[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=4[N:6]=[CH:5][C:4]=3[C:3]2=[O:14])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 6115AnilineHCID 57183566Furo[3,4-c]quinolin-3(1H)-one

Product 1

HCID 57023940HCID 57023940, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

A mixture Furo[3,4-c]quinolin-3(1H)-one (100 mg) and aniline (2 mL) was heated at 180° C. for 5 min. After cooling to room temperature the mixture was slowly diluted with hexane and the resulting product was collected and washed with hexane to afford 2-Phenyl-pyrrolo[3,4-c]quinolin-3(1H)-one.

Workup

  1. customthe resulting product was collected
  2. washwashed with hexane

Sources & evidence

ORD record
ord-273c5eb135a04e95a9a37fa897521272
Source dataset
uspto-grants-1993_09
Patent number
US05243049

Reaction notes

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