HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → HCID 68183413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | Quinoline, 7-(1-methylethyl)-8-nitro- | HCID 68183428 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 68183413 | HCID 68183413 | 73% |
Reaction Steps
In a similar fashion using route 1 general procedure 4, 7-isopropyl-8-nitroquinoline (Intermediate 59) (670 mg, 3.09 mmol), tin (II) chloride (1.8 g, 9.3 mmol) and 6 N HCl (6 drops) gave the title compound (420 mg, 73%) which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-8eebe95e20494ca6a8ff315fb8772986 |
| Source note | uspto-grants-2015_08 |