HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-Aminoquinoline → HCID 22974334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-Aminoquinoline | HCID 11359 | — |
| Reactant | Pyridine-2-sulfonyl Chloride | HCID 3787675 | — |
| Product | HCID 22974334 | HCID 22974334 | 66% |
Reaction Steps
In a similar fashion using route 14 general procedure 26, 8-aminoquinoline (100 mg, 0.69 mmol), pyridine-2-sulfonyl chloride (Intermediate 18) (196 mg, 1.107 mmol) gave the title compound (130 mg, 65%) after purification by column chromatography with n-hexane/EtOAc (17:3) as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f4db456bd3274f6ba834038bf42af260 |
| Source note | uspto-grants-2015_08 |