HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 60163841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 8-Quinolinamine, 6-methyl- | HCID 110237 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 60163841 | HCID 60163841 | 61% |
Reaction Steps
In the similar fashion using route 14 general procedure 27, 3-methylquinoline (Intermediate 31) (130 mg, 0.82 mmol), benzenesulfonyl chloride (170 mg, 0.9 mmol) and DMAP (cat.) gave the title compound (150 mg, 61%) after tituration from n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-b0ffd27a24a34d0e9ddee18ad2172fa5 |
| Source note | uspto-grants-2015_08 |