HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → 2-Amino-4,5-dimethyl-N-quinolin-8-yl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 4,5-dimethyl-2-nitro-N-quinolin-8-yl-benzenesulfonamide | HCID 68183463 | — |
| Product | 2-Amino-4,5-dimethyl-N-quinolin-8-yl-benzenesulfonamide | HCID 68183391 | 66% |
Reaction Steps
In a similar fashion using route 15 general procedure 29, 4,5-dimethyl-2-nitro-N-quinolin-8-yl-benzenesulfonamide (Intermediate 147) (0.52 g, 1.45 mmol) and tin (II) chloride dihydrate (1.37 g, 7.26 mmol) gave the title compound (0.31 g, 66%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-40a2673145544a35992358d1fcf3b5ad |
| Source note | uspto-grants-2015_08 |