HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 68183175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 68183167 | HCID 68183167 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68183175 | HCID 68183175 | 63% |
Reaction Steps
In the similar fashion using route 15 general procedure 29, N-(5-chloro-quinolin-8-yl)-4-methanesulfonyl-2-nitro-benzenesulfonamide (Intermediate 262 (350 mg, 0.79 mmol), SnCl2 (399 mg, 4.76 mmol) and EtOH (12 ml) gave the title compound (205 mg, 63%) after trituration from DCM: pentane
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d4ec9429b03c4770a53d19ec8ddc3d8c |
| Source note | uspto-grants-2015_08 |