HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → HCID 86669761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 86669757 | HCID 86669757 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86669761 | HCID 86669761 | 80.3% |
Reaction Steps
In a similar fashion using route 1 general procedure 4, N-(2-chloro-quinolin-8-yl)-2-nitro-benzenesulfonamide (Intermediate 255) (0.80 g, 2.2 mmol), SnCl2 (1.7 g, 8.8 mmol), 6N HCl (2 drops) and EtOH (15 ml) gave the title compound (0.59 g, 80%) which was used in the next steps without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-38ea20694d074fbcb0f03eebbb156e89 |
| Source note | uspto-grants-2015_08 |