HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → HCID 68183117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 68183041 | HCID 68183041 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68183117 | HCID 68183117 | 74.9% |
Reaction Steps
In a similar fashion using route 1 general procedure 4, 2-nitro-N-quinolin-8-yl-5-trifluoromethyl-benzenesulfonamide (Intermediate 270) (490 mg, 1.2 mmol), SnCl2 (936 mg, 4.93 mmol), 6N HCl (5 drops) and EtOH (10 ml) gave the title compound (330 mg, 73%) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-ed7a6bfeace940f1a7790927b331e784 |
| Source note | uspto-grants-2015_08 |