Acetic Acid → HCID 68183025, compound

Participants

Reaction Steps

In a similar fashion using route 16 general procedure 61, 2-amino-N-benzothiazol-4-yl-benzenesulfonamide (Intermediate 289) (190 mg, 0.62 mmol), t-butyl nitrite (96 mg, 0.93 mmol), AcOH (1.9 ml) and THF (4 ml) gave the title compound (35 mg, 19.5%) after purification by column chromatography with DCM/MeOH (99:1) as the eluent.

Provenance & Evidence