Cornforth reagent → HCID 68183178, compound

Participants

Reaction Conditions

Reaction Steps

PDC (404 mg, 1.08 mmol) was added to a solution of (4-fluoro-phenyl)-(8-nitro-quinolin-7-yl)-methanol (Intermediate 337) (214 mg, 0.72 mmol) in DCM (10 ml). The mixture was heated to 30° C. and stirring was continued for 18 h. After cooling, the mixture was concentrated in vacuo. The crude residue was dissolved in toluene, filtered and concentrated in vacuo to give the title compound (160 mg, 75%).

Provenance & Evidence