HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 20609053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-5-methyl-pyridine | HCID 581393 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 20609053 | HCID 20609053 | 72.8% |
Reaction Steps
In a similar fashion using route 38 general procedure 92, 2-chloro-5-methyl pyridine (200 mg, 1.5 mmol), K2CO3 (325 mg, 2.3 mmol), benzylmercaptan (292 mg, 2.3 mmol) and DMSO (1.5 ml) at 150° C. for 4 h gave the title compound (235 mg, 69%) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-1b954ab56f7d4f84a9be19bccdb7bf42 |
| Source note | uspto-grants-2015_08 |