HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 79018155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21291171 | HCID 21291171 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 79018155 | HCID 79018155 | — |
Reaction Steps
In a similar fashion using route 39 general procedure 96, 5-methoxy-2-nitro-benzenesulfonic acid 447 (2.0 g, 8.58 mmol), SOCl2 (9.4 ml) and (0.2 ml) DMF gave the title compound (2.5 g) which was used in the next step without further purification. The structure was confirmed by 1H NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-5050f10cbe9b4fcf92d2e9082a6f86ca |
| Source note | uspto-grants-2015_08 |