HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 157915-10-1
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-Quinolinecarboxylic acid | HCID 10243 | — |
| Product | Sulfuric Acid | HCID 1118 | — |
| Product | 157915-10-1 | HCID 1239827 | 106% |
| Product | HCID 14226197 | HCID 14226197 | — |
Reaction Steps
In a similar fashion using route 11 general procedure 15, 4-carboxyquinoline (1.6 g, 9.0 mmol) in conc. H2SO4 (3 ml) and fuming HNO3/conc. H2SO4 (1:1; 6 ml) to give the title compound and 4-carboxy-5-nitroquinoline (2.1 g, 106%) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-02ded989f2fe4310a39c5971f8267f88 |
| Source note | uspto-grants-2015_08 |