HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 68183334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 68183202 | HCID 68183202 | — |
| Product | HCID 68183334 | HCID 68183334 | 50% |
Reaction Steps
In a similar fashion using route 53 general procedure 122, 8-benzenesulfonylamino-quinoline-4-carboxylic acid methyl ester 225 (50 mg, 0.15 mmol) and methyl amine (33% in EtOH, 3 ml) gave the title compound (23 mg, 50%) after purification by column chromatography with DCM/MeOH (95:5) as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-00683cc518fe4367932a3525053448bd |
| Source note | uspto-grants-2015_08 |