HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 5-(Benzyloxy)quinolin-8-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 5-Benzyloxy-8-nitro-quinoline | HCID 68183258 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(Benzyloxy)quinolin-8-amine | HCID 43449587 | 66% |
Reaction Steps
In a similar fashion using route 19 general procedure 29, 5-benzyloxy-8-nitro-quinoline 564 (572 mg, 2.04 mmol), SnCl2 (1.84 g, 8.16 mmol), and EtOH (15 ml) gave the title compound (336 mg, 66%) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-3c58f6813a8a46d683181b3daf2f4b99 |
| Source note | uspto-grants-2015_08 |