HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → N*7*-Phenyl-quinoline-7,8-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 68183224 | HCID 68183224 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N*7*-Phenyl-quinoline-7,8-diamine | HCID 131733285 | 64.3% |
Reaction Steps
In a similar fashion using route 19 general procedure 29, (8-nitro-quinolin-7-yl)-phenyl-amine 574 (100 mg, 0.37 mmol), SnCl2 (425 mg, 1.8 mmol) and EtOH (10 ml) gave the title compound (56 mg, 62%) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102688B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-188e9b9a32a94ddab61bf168c29a9716 |
| Source note | uspto-grants-2015_08 |