Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4'-Methoxyacetophenone → (2E)-3-(dimethylamino)-1-(4-methoxyphenyl)prop-2-en-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4'-Methoxyacetophenone | HCID 7476 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | (2E)-3-(dimethylamino)-1-(4-methoxyphenyl)prop-2-en-1-one | HCID 5397461 | 88% |
반응 단계
The title compound was prepared in 88% yield from 1-(4-methoxyphenyl)ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.88-3.06 (6H, br s), 3.85 (3H, s), 5.71 (1H, d, J=12.0 Hz), 6.91 (2H, d, J=8.8 Hz), 7.84 (1H, d, J=12.0 Hz), 7.91 (2H, d, J=8.8 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09107916B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-5aa013ad1703493197f77f9d568a5352 |
| 출처 메모 | uspto-grants-2015_08 |