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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 514355Generated: October 29, 2026

Dimethylformamide dimethyl acetal → HCID 86725492, compound

https://huagongshe.com/reaction/514355

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
Reactant4-MethylsulfonylacetophenoneHCID 82529—
ProductHCID 86725492HCID 8672549287%

Reaction Steps

The title compound was prepared in 87% yield from 1-[4-(methylsulfonyl)phenyl]ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.96 (3H, s), 3.06 (3H, s), 3.19 (3H, s), 5.66 (1H, d, J=12 Hz), 7.83 (1H, d, J=12 Hz), 7.96-8.04 (4H, m).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09107916B2
Source datasetuspto-grants-2015_08
ORD IDord-901961b206884366904ab1068c5b5057
Source noteuspto-grants-2015_08