HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69781884, compound → HCID 86725624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69781884 | HCID 69781884 | — |
| Reactant | HCID 178510213 | HCID 178510213 | — |
| Product | HCID 86725624 | HCID 86725624 | — |
Reaction Steps
The title compound was prepared from 2-(5-hydroxy-1H-pyrazol-1-yl)pyridine-4-carbonitrile and (2-ethyl-4-fluorophenyl)methanol according to the procedure for the preparation of Example 39, part C. 1H NMR (400 MHz, CDCl3): δ 1.23 (3H, t, J=7.6 Hz), 2.72 (2H, q, J=7.6 Hz), 5.20 (2H, s), 5.79 (1H, d, J=2.0 Hz), 6.89-7.00 (2H, m), 7.36-7.40 (2H, m), 7.59 (1H, d, J=2.0 Hz), 7.98 (1H, s), 8.67 (1H, d, J=5.2 Hz). [M+H] Calc'd for C18H15FN4O, 323. Found, 323.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107916B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-3d5f945aa69a49d182c1c95f611a85f3 |
| Source note | uspto-grants-2015_08 |