HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 84652366, compound → HCID 86725660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 84652366 | HCID 84652366 | — |
| Reactant | HCID 178510213 | HCID 178510213 | — |
| Product | HCID 86725660 | HCID 86725660 | — |
Reaction Steps
The title compound was prepared from 2-(5-hydroxy-1H-pyrazol-1-yl)pyridine-4-carbonitrile and (4-cyclopropyl-3-fluorophenyl)methanol according to the procedure for the preparation of Example 39, part C. 1H NMR (400 MHz, CDCl3): δ 0.71-0.75 (2H, m), 0.96-1.02 (2H, m), 2.06-2.10 (1H, m), 5.17 (2H, s), 5.72 (1H, d, J=1.6 Hz), 6.88-6.92 (1H, m), 7.07-7.10 (2H, m), 7.40 (1H, dd, J=1.6 Hz, 5.2 Hz), 7.55 (1H, d, J=2.0 Hz), 8.02 (1H, s), 8.70 (1H, d, J=5.2 Hz). [M+H] Calc'd for C19H15FN4O, 335. Found, 335.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107916B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-bef2ae1dabb146d6980cc2f0540b7f53 |
| Source note | uspto-grants-2015_08 |