HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorophenylacetic acid → HCID 26597788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorophenylacetic acid | HCID 123585 | — |
| Reactant | Potassium methyl malonate | HCID 2724687 | — |
| Product | HCID 26597788 | HCID 26597788 | — |
Reaction Steps
The title compound was prepared from 2-(2,6-difluorophenyl)acetic acid and 3-methoxy-3-oxopropanoic acid potassium salt according to the procedure for the preparation of Example 170, part A. 1H NMR (300 MHz, CDCl3): δ 3.56 (2H, s), 3.75 (3H, s), 3.92 (2H, s), 6.89-6.93 (2H, m), 7.22-7.27 (1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107916B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-b456552adedc472da14de72c70b460e1 |
| Source note | uspto-grants-2015_08 |