HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyl-1,3-dioxane-4,6-dione → Ethyl 4-(2-chlorophenyl)-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Reactant | o-Chlorophenylacetic acid | HCID 17124 | — |
| Product | Ethyl 4-(2-chlorophenyl)-3-oxobutanoate | HCID 13069496 | 43% |
Reaction Steps
The title compound was prepared in 43% yield from 2-(2-chlorophenyl)acetic acid and 2,2-dimethyl-1,3-dioxane-4,6-dione according to the procedure for the preparation of Example 162, part A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107916B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-b525cad03ec94deb88c84aa7b35c9148 |
| Source note | uspto-grants-2015_08 |