HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenylacetic acid → ethyl 4-(3-chlorophenyl)-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenylacetic acid | HCID 15879 | — |
| Reactant | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| Product | ethyl 4-(3-chlorophenyl)-3-oxobutanoate | HCID 10538052 | 43% |
Reaction Steps
The title compound was prepared in 43% yield from 2-(3-chlorophenyl)acetic acid and 2,2-dimethyl-1,3-dioxane-4,6-dione according to the procedure for the preparation of Example 162, part A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09107916B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-9de20536820646be8e2762fe8b681278 |
| Source note | uspto-grants-2015_08 |