HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-acetamidoacrylate → HCID 118023697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-acetamidoacrylate | HCID 98644 | — |
| Reactant | 3-Hydrazinylpyridine dihydrochloride | HCID 17132489 | — |
| Reactant | 3-(3-chloro-1H-pyrazol-1-yl)pyridine | HCID 67499540 | — |
| Product | HCID 118023697 | HCID 118023697 | — |
Reaction Steps
3-(3-Chloro-1H-pyrazol-1-yl)pyridine (5b) in Scheme 1 may alternatively be prepared by reacting 3-hydrazinopyridine dihydrochloride with methyl 2-acetamidoacrylate to yield N-(3-oxo-1-(pyridin-3-yl)pyrazolidin-4-yl)acetamide and subsequent chlorination/elimination as shown in Scheme 2, step a1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108946B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-621e3718b13947ccb64d5f375e03f7c6 |
| Source note | uspto-grants-2015_08 |