HCID 68611887, compound → HCID 86671003, compound

Participants

Reaction Steps

tert-Butyl 4-(5-nitro-1H-indol-1-yl)piperidine-1-carboxylate (9.04 mmol, 3.123 g) and 10% palladium on carbon (0.452 mmol, 0.481 g) were combined and stirred under a hydrogen atmosphere at 5 bar at room temperature in ethanol (25 mL) for 1 hour. The reaction mixture was filtered and concentrated at reduced pressure to afford the title compound. (2.506 g). MS (ESI) m/z 316.1 [M+H]+

Provenance & Evidence