HuagongsheHuagongshe Chemistry Print Report · For research reference only
DL-cysteine → HCID 58329594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | DL-cysteine | HCID 594 | — |
| Reactant | HCID 67251754 | HCID 67251754 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 58329594 | HCID 58329594 | — |
Reaction Steps
To a solution of D,L-cysteine (0.056 g, 0.460 mmol) in TFA (0.9 mL) was added tert-butyl 2-(7-(4-chloro-3-(trifluoromethyl)benzyloxy)-2,3-dihydro-1H-pyrrolo[1,2-a]indol-1-yl)acetate (0.079 g, 0.153 mmol). The reaction was stirred for 2 h and poured into ice water. The resulting precipitate was collected by vacuum filtration to give the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09108969B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f942bf8f7d3a45c7bd163f00fee59296 |
| Source note | uspto-grants-2015_08 |