HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15172910, compound → HCID 87082349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15172910 | HCID 15172910 | — |
| Reactant | N-(3-(3-bromophenyl)-3-hydroxypropyl)-2,2,2-trifluoroacetamide | HCID 57608426 | — |
| Product | HCID 87082349 | HCID 87082349 | — |
Reaction Steps
Sonogashira reaction of 25 with but-3-ynyl-cyclopentane yielded N-(3-(3-(4-cyclopentylbut-1-ynyl)phenyl)-3-hydroxypropyl)-2,2,2-trifluoroacetamide as a dark brown oil. Yield (690 mg, 69%): 1H NMR (400 MHz, CDCl3) δ 7.22-7.57 (m, 4H),
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115056B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f9806f22a28a402b9c27f21fe192cb41 |
| Source note | uspto-grants-2015_08 |