HRID517222

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12290550

未命名化合物

结构：Cc1cc(C#N)ccc1N(CC1=C(Nc2cccc(C(F)(F)F)c2)CCCC1=O)C(=O)OC(C)(C)C

HCID86732339

未命名化合物

2 次

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)N(CC1=C(Nc2cccc(C(F)(F)F)c2)CCCC1=O)c1ccc(C#N)cc1Cl

HCID86732342

未命名化合物

PROCEDURE

实验过程

The title compound is prepared in analogy to tert-butyl (4-cyano-2-methylphenyl)(6-oxo-2-(3-(trifluoromethyl)phenylamino)cyclohex-1-enyl)methylcarbamate (intermediate 51), using 3-chloro-4-formylbenzonitrile (500 mg, 6.04 mmol) as starting material. Yield: 1.05 g; ESI mass spectrum [M+H]+=520; Retention time HPLC: 0.81 min (X012_S01).

WORKUP

后处理

custom0.81 min (X012_S01)