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HRID517286

反应详情

EQUATION

反应方程式

HRID 517286 的结构方程式

REACTANTS

反应物

2
结构：CCN
HCID6341

Ethanamine

C2H7N

结构：CNC(=O)N1C(=O)N(c2cccc(C(F)(F)F)c2)C2=C(C(=O)CCC2)C1c1ccc(C#N)cc1C
HCID86732412

未命名化合物

PRODUCTS

生成物

1
结构：CCNC(=O)N1C(=O)N(c2cccc(C(F)(F)F)c2)C2=C(C(=O)CCC2)C1c1ccc(C#N)cc1C
HCID86732413

未命名化合物

PROCEDURE

实验过程

The title compound is prepared in analogy to 4-(4-cyano-2-methylphenyl)-N-methyl-2,5-dioxo-1-(3-(trifluoromethyl)phenyl)-1,2,5,6,7,8-hexahydroquinazoline-3(4H)-carboxamide (example 73), replacing methylamine with ethylamine as reagent. Yield: 45 mg; ESI mass spectrum [M+H]+=497; Retention time HPLC: 0.77 min (X012_S01).

WORKUP

后处理

  1. custom0.77 min (X012_S01)