Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → (2E)-3-[5-(benzyloxycarbonyl)furan-2-yl]-2-propenoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | 5-(2-tert-Butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester | HCID 77934550 | — |
| 생성물 | (2E)-3-[5-(benzyloxycarbonyl)furan-2-yl]-2-propenoic acid | HCID 70869499 | — |
반응 단계
To 5-(2-tert-butoxycarbonylethenyl)furan-2-carboxylic acid benzyl ester (0.15 g, 0.46 mmol) obtained in Example 41, step 2 was added trifluoroacetic acid (3 mL), and the mixture was stirred for 30 minutes. The solvent was evaporated under reduced pressure to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09115107B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-f491899c07b74235a3fb6af232a38953 |
| 출처 메모 | uspto-grants-2015_08 |