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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 517338Generated: October 30, 2026

HCID 70869504, compound → HCID 68320279, compound

https://huagongshe.com/reaction/517338

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70869504HCID 70869504—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
SolventChloroformHCID 6212—
ProductHCID 68320279HCID 68320279—

Reaction Steps

The compound (0.5 g, 1.45 mmol) obtained in step 1 was dissolved in methanol (5 mL) and chloroform (0.5 mL), palladium hydroxide (0.1 g) was added, and the mixture was stirred at room temperature overnight under a hydrogen atmosphere. The reaction mixture was filtered through celite, and the solvent was evaporated under reduced pressure to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09115107B2
Source datasetuspto-grants-2015_08
ORD IDord-518c9929e7d84cd7a6d33b81557f49d4
Source noteuspto-grants-2015_08