HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethanol → HCID 71697658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethanol | HCID 34 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Diisopropyl azodicarboxylate | HCID 5363146 | — |
| Reactant | (Z)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione | HCID 5878179 | — |
| Product | HCID 71697658 | HCID 71697658 | — |
Reaction Steps
The title compound 28f was prepared from compound 2 (249 mg, 1.00 mmol), 2-chloroethanol (100 μL, 1.50 mmol), triphenylphosphine (393 mg, 1.50 mmmol) and DIAD (295 μL, 1.50 mmol) in a manner similar to that described for 9 in 88.5% (276 mg) yield as a light-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115122B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-af139269a70c4e1b826f98d7bbf71078 |
| Source note | uspto-grants-2015_08 |