Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 23932524 | HCID 23932524 | — |
| Product | HCID 44159093 | HCID 44159093 | — |
Reaction Steps
A mixture of ethyl 3-(1,2,3,4-tetrahydro-2,8-dimethylpyrido[4,3-b]indol-5-yl)propanoate (100 mg, 0.33 mmol) and ethyl amine (40% aq, 2.5 ml) was heated at 100-120° C. for 3-4 h to obtain 19 mg of N-ethyl-3-(1,2,3,4-tetrahydro-2,8-dimethylpyrido[4,3-b]indol-5-yl)propanamide after purification on neutral alumina chromatography eluting with methanol-dichloromethane gradient.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09115137B2 |
|---|
| Source dataset | uspto-grants-2015_08 |
|---|
| ORD ID | ord-97faa8e8565d47c7920dfc348ef22909 |
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| Source note | uspto-grants-2015_08 |
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