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HRID517828

反应详情

EQUATION

反应方程式

HRID 517828 的结构方程式

REACTANTS

反应物

2
结构：CCN
HCID6341

Ethanamine

C2H7N

结构：CCOC(=O)CCCn1c2c(c3cc(C)ccc31)CN(C)CC2
HCID44159096

未命名化合物

PRODUCTS

生成物

1
结构：CCNC(=O)CCCn1c2c(c3cc(C)ccc31)CN(C)CC2
HCID44159097

未命名化合物

PROCEDURE

实验过程

Ethyl 4-(1,2,3,4-tetrahydro-2,8-dimethylpyrido[4,3-b]indol-5-yl)butanoate (80 mg, 0.2 mmol) was stirred with ethylamine (0.8 ml) at 100-120° C. for 3-4 h to obtain 40 mg of N-ethyl-4-(1,2,3,4-tetrahydro-2,8-dimethylpyrido[4,3-b]indol-5-yl)butanamide after purification on neutral alumina chromatography eluting with methanol-dichloromethane gradient.