HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonamide → US10023592, Example 166
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | US10023592, Example 149 | HCID 118022283 | — |
| Product | US10023592, Example 166 | HCID 118022553 | — |
Reaction Steps
The title compound of Example 149, step 4 was treated with MeSO2NH2 in a manner similar to Example 152, step 6 to give the title compound. 1H NMR (CDCl3, 400 MHz) δ 8.42 (s, 1H), 8.36 (s, 1H), 8.10-8.12 (m, 2H), 6.98-7.05 (m, 2H), 6.87-6.92 (m, 1H), 3.64 (s, 3H), 3.45 (s, 3H), 2.22 (s, 3H). LCMS: 423.0 (M+1)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115114B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-bf0639d1af0e4f219a789e17f1f31d21 |
| Source note | uspto-grants-2015_08 |