HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-bromo-4-(2,4-difluorophenoxy)phenyl)ethanesulfonamide → US10023592, Example 281
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-bromo-4-(2,4-difluorophenoxy)phenyl)ethanesulfonamide | HCID 117770988 | — |
| Reactant | N-[3-bromo-4-(2,4-difluorophenoxy)phenyl]methanesulfonamide | HCID 118022469 | — |
| Reactant | 3-Fluoro-1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-one | HCID 123823790 | — |
| Product | US10023592, Example 281 | HCID 118022534 | — |
Reaction Steps
The title compound was prepared in a manner similar to Example 122, substituting 1-methyl-3-pyrrolidin-1-yl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-one for 3-Fluoro-1-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-one and N-[3-bromo-4-(2,4-difluorophenoxyl)phenyl]methanesulfonamide for N-[3-Bromo-4-(2,4-difluorophenoxyl)phenyl]ethanesulfonamide. LCMS (M+H)+=476.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09115114B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-757779ef60574c9eaad2ec366c675fee |
| Source note | uspto-grants-2015_08 |