O-Methylhydroxylamine → HCID 178454594, compound

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Reaction Steps

The title compound was prepared from cis-4-((E)-2-(4-fluorobenzoylimino)-6-(morpholinomethyl)-2,3-dihydro-1H-benzo[d]imidazol-1-yl)cyclohexanecarbonyl chloride and O-methylhydroxylamine using a method analogous to that used in the preparation of (E)-4-fluoro-N-(1-(cis-4-(1-hydroxy-2-methylpropan-2-ylcarbamoyl)cyclohexyl)-6-(morpholinomethyl)-1H-benzo[d]imidazol-2(3H)-ylidene)benzamide (27.4 mg, 54% yield). MS, m/z (C27H32FN5O4): calcd, 509.2. found, 510.2 [M+H].

Provenance & Evidence