Methacrylic anhydride → 2-[Ethyl(phenyl)amino]ethyl prop-2-enoate

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

Methacrylic anhydride (7.7 g, 0.05 mol) is added to a solution of N-(2-hydroxyethyl)-N-ethylaniline (6.6 g, 0.04 mol) in pyridine (25 ml) and the mixture is stirred at 55° C. for 2 hours. On cooling the mixture is passed through silica gel to give N-(2-acryloyloxyethyl)-N-ethylaniline as a pale yellow oil. 5.3 g, 65%

Herkunft & Nachweise