Benzylamine → HCID 58946770, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 112b (20g, 38.8 mmol) in toluene (100 ml) was added BnNH2 (12.48g, 116.5 mmol). The reaction mixture was stirred at 90° C. for 3h. Then the mixture was purified through a silica gel column eluting with PE:EA=50:1 to 10:1 to give 112c as a white crystal (10.7g, 60%) MS: [M+H]+: 461

Provenance & Evidence