1-(2,3-Xylyl)piperazine → HCID 56944107, compound
Reaction equation
F[C:2](F)(F)[C:3]1[CH:4]=[C:5]([N:9]2[CH2:14][CH2:13][N:12]([CH2:15][CH2:16][N:17]3[C:26](=[O:27])[C:25]4[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=4)[N:19]=[CH:18]3)[CH2:11][CH2:10]2)[CH:6]=[CH:7][CH:8]=1.[CH3:30]C1C(C)=CC=CC=1N1CCNCC1>>[CH3:30][C:4]1[C:3]([CH3:2])=[CH:8][CH:7]=[CH:6][C:5]=1[N:9]1[CH2:10][CH2:11][N:12]([CH2:15][CH2:16][N:17]2[C:26](=[O:27])[C:25]3[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=3)[N:19]=[CH:18]2)[CH2:13][CH2:14]1Participants
3
Procedure
This compound was prepared in compliance with the procedure described in 1c, using 1-(2,3-dimethylphenyl)piperazine instead of 1-(3-(trifluoromethyl)phenyl)piperazine.
Workup
- customThis compound was prepared in compliance with the procedure
Sources & evidence
- ORD record
- ord-677df73deb7e4e518b154a85739743fa
- Source dataset
- uspto-grants-2016_05
- Patent number
- US09326984B2
Reaction notes
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