HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-(methylthio)aniline → N-[5-chloro-2-(methylthio)phenyl]-1-benzofuran-2-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Reactant | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| Product | N-[5-chloro-2-(methylthio)phenyl]-1-benzofuran-2-sulfonamide | HCID 57378529 | 60% |
Reaction Steps
Following General Procedure B, the title compound (243 mg, 60%) was prepared from 5-chloro-2-(methylthio)aniline (CAS 16423-54-4) (200 mg, 1.15 mmol) and 1-benzofuran-2-sulfonyl chloride (249 mg, 1.152 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-992d6ea592ed4a57a07a1c9345a96a98 |
| Source note | uspto-grants-2016_05 |