Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Benzofuran-2-sulfonyl chloride → N-(5-chloro-2-{[2-(1H-pyrazol-4-yl)ethyl]thio}phenyl)-1-benzofuran-2-sulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| 반응물 | 2-((2-(1H-pyrazol-4-yl)ethyl)thio)-5-chloroaniline | HCID 67972877 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | N-(5-chloro-2-{[2-(1H-pyrazol-4-yl)ethyl]thio}phenyl)-1-benzofuran-2-sulfonamide | HCID 67972412 | 45.9% |
반응 단계
Following General Procedure B, the title compound (123 mg) was prepared from 2-((2-(1H-pyrazol-4-yl)ethyl)thio)-5-chloroaniline (157 mg, 0.618 mmol) and benzofuran-2-sulfonyl chloride (133 mg, 0.618 mmol) in pyridine (3 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09328067B2 |
| 출처 데이터셋 | uspto-grants-2016_05 |
| ORD ID | ord-a9640d34bdc041b0b003cf1f05f8fb13 |
| 출처 메모 | uspto-grants-2016_05 |